TA Instruments

AR1770-0002f

28/03/2013 11:04:27

Sample name	DI 40 mm AL P120B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1770
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 11:04:27

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	4.841	-151.00	10000	20.0	5.881	31.000	-12.02	9.682	-1.241	9360	2.3644	99.85	4.7287	472.87	3.411E-3	0.0	0.5
2.0240	10.22	13.374	10000	20.0	5.874	32.024	1.064	20.44	0.05206	9349	13.8559	22.37	27.712	2771.2	3.411E-3	0.0	0.5
3.0000	15.68	24.390	10000	20.0	5.877	33.000	1.941	31.37	0.06188	9353	27.5037	9.507	55.007	5500.7	3.411E-3	0.1	0.6
4.0000	18.59	31.812	10000	20.0	5.873	34.000	2.532	37.18	0.06808	9347	41.4258	6.761	82.852	8285.2	3.411E-3	0.1	0.6
5.0000	24.79	48.882	10000	20.0	5.877	35.000	3.890	49.59	0.07844	9353	68.1910	3.803	136.38	13638	3.411E-3	0.1	0.6
6.0200	31.68	71.689	10000	20.0	5.871	36.020	5.705	63.36	0.09004	9344	107.2550	2.328	214.51	21451	3.411E-3	0.1	0.6
7.0000	34.11	79.773	10000	20.0	5.868	37.000	6.348	68.23	0.09304	9340	127.4260	2.006	254.85	25485	3.411E-3	0.1	0.6
8.0000	39.37	99.729	10000	20.0	5.865	38.000	7.936	78.74	0.1008	9335	165.9390	1.506	331.88	33188	3.411E-3	0.1	0.6
9.0000	46.08	128.31	10000	20.0	5.862	39.000	10.21	92.16	0.1108	9330	223.6170	1.099	447.23	44723	3.411E-3	0.2	0.7
10.000	51.00	151.52	10000	20.0	5.861	40.000	12.06	102.0	0.1182	9328	275.1460	0.8966	550.29	55029	3.411E-3	0.2	0.7
11.000	55.76	175.77	10000	20.0	5.855	41.000	13.99	111.5	0.1254	9318	326.4530	0.7492	652.91	65291	3.411E-3	0.2	0.7
12.024	60.13	199.31	10000	20.0	5.846	42.024	15.86	120.3	0.1319	9304	377.6350	0.6433	755.27	75527	3.411E-3	0.2	0.7
13.012	64.44	222.98	10000	20.0	5.844	43.012	17.74	128.9	0.1377	9301	435.2660	0.5599	870.53	87053	3.411E-3	0.2	0.7
14.000	69.18	252.10	10000	20.0	5.839	44.000	20.06	138.4	0.1450	9293	499.0380	0.4855	998.08	99808	3.411E-3	0.2	0.7
15.000	75.71	293.91	10000	20.0	5.830	45.000	23.39	151.4	0.1545	9279	594.5860	0.4047	1189.2	1.1892E5	3.411E-3	0.3	0.8
16.004	79.95	320.82	10000	20.0	5.823	46.004	25.53	159.9	0.1597	9267	664.6250	0.3624	1329.3	1.3293E5	3.411E-3	0.3	0.8
17.000	84.55	355.89	10000	20.0	5.819	47.000	28.32	169.1	0.1675	9260	740.9940	0.3238	1482.0	1.4820E5	3.411E-3	0.3	0.8
18.016	91.00	386.54	10000	20.0	5.807	48.016	30.76	182.0	0.1690	9243	859.9680	0.2790	1719.9	1.7199E5	3.411E-3	0.3	0.8
19.020	95.05	431.50	10000	20.0	5.807	49.020	34.34	190.1	0.1806	9242	931.4960	0.2557	1863.0	1.8630E5	3.411E-3	0.3	0.8
20.016	99.41	465.72	10000	20.0	5.798	50.016	37.06	198.8	0.1864	9227	1020.8200	0.2334	2041.6	2.0416E5	3.411E-3	0.3	0.8
21.016	105.8	517.19	10000	20.0	5.786	51.016	41.16	211.7	0.1944	9208	1153.6801	0.2055	2307.4	2.3074E5	3.411E-3	0.4	0.9
22.000	109.9	551.09	10000	20.0	5.775	52.000	43.85	219.8	0.1995	9192	1243.3400	0.1902	2486.7	2.4867E5	3.411E-3	0.4	0.9
23.000	114.2	591.45	10000	20.0	5.770	53.000	47.07	228.5	0.2060	9184	1343.8500	0.1759	2687.7	2.6877E5	3.411E-3	0.4	0.9
24.016	120.7	647.02	10000	20.0	5.758	54.016	51.49	241.3	0.2133	9165	1496.2400	0.1574	2992.5	2.9925E5	3.411E-3	0.4	0.9
25.000	124.7	688.81	10000	20.0	5.745	55.000	54.81	249.5	0.2197	9144	1597.3000	0.1469	3194.6	3.1946E5	3.411E-3	0.4	0.9
26.000	129.1	735.02	10000	20.0	5.730	56.000	58.49	258.1	0.2266	9120	1711.3700	0.1369	3422.7	3.4227E5	3.411E-3	0.4	0.9
27.004	135.5	802.51	10000	20.0	5.719	57.004	63.86	270.9	0.2357	9102	1882.2600	0.1240	3764.5	3.7645E5	3.411E-3	0.5	1.0
28.000	139.6	861.01	10000	20.0	5.702	58.000	68.52	279.1	0.2455	9076	1996.1400	0.1165	3992.3	3.9923E5	3.411E-3	0.5	1.0
29.000	143.6	901.13	10000	20.0	5.690	59.000	71.71	287.3	0.2496	9056	2116.9500	0.1097	4233.9	4.2339E5	3.411E-3	0.5	1.0
30.000	150.1	995.62	10000	20.0	5.673	60.000	79.23	300.1	0.2640	9029	2306.1399	0.1002	4612.3	4.6123E5	3.411E-3	0.5	1.0
31.016	154.2	1046.2	10000	20.0	5.654	61.016	83.26	308.3	0.2700	8999	2432.6599	0.09466	4865.3	4.8653E5	3.411E-3	0.5	1.0
32.020	160.4	1137.0	10000	20.0	5.625	62.020	90.48	320.8	0.2820	8953	2635.8799	0.08697	5271.8	5.2718E5	3.411E-3	0.5	1.0
33.000	164.7	1178.9	10000	20.0	5.608	63.000	93.81	329.4	0.2848	8925	2779.9099	0.08227	5559.8	5.5598E5	3.411E-3	0.6	1.1
34.016	168.8	1254.6	10000	20.0	5.591	64.016	99.84	337.6	0.2958	8898	2912.9500	0.07809	5825.9	5.8259E5	3.411E-3	0.6	1.1
35.000	174.9	1350.2	10000	20.0	5.556	65.000	107.4	349.8	0.3072	8842	3127.8501	0.07228	6255.7	6.2557E5	3.411E-3	0.6	1.1
36.004	179.1	1405.7	10000	20.0	5.539	66.004	111.9	358.2	0.3123	8815	3280.2400	0.06869	6560.5	6.5605E5	3.411E-3	0.6	1.1
37.024	183.3	1471.3	10000	20.0	5.517	67.024	117.1	366.5	0.3194	8781	3509.0200	0.06536	7018.0	7.0180E5	3.411E-3	0.6	1.1
38.000	189.3	1573.7	10000	20.0	5.487	68.000	125.2	378.6	0.3307	8732	3665.1799	0.06091	7330.4	7.3304E5	3.411E-3	0.6	1.1
39.000	193.5	1636.5	10000	20.0	5.471	69.000	130.2	386.9	0.3366	8707	3822.4700	0.05816	7644.9	7.6449E5	3.411E-3	0.7	1.2
40.016	199.7	1741.7	10000	20.0	5.442	70.016	138.6	399.4	0.3470	8661	4068.7600	0.05430	8137.5	8.1375E5	3.411E-3	0.7	1.2
41.016	203.7	1808.6	10000	20.0	5.403	71.016	143.9	407.4	0.3533	8599	4232.8901	0.05181	8465.8	8.4658E5	3.411E-3	0.7	1.2
42.020	210.0	1931.8	10000	20.0	5.380	72.020	153.7	419.9	0.3661	8563	4498.8799	0.04856	8997.8	8.9978E5	3.411E-3	0.7	1.2
43.000	214.1	1996.7	10000	20.0	5.367	73.000	158.9	428.2	0.3711	8542	4674.7598	0.04659	9349.5	9.3495E5	3.411E-3	0.7	1.2
44.008	218.1	2081.6	10000	20.0	5.348	74.008	165.6	436.3	0.3797	8511	4852.5498	0.04472	9705.1	9.7051E5	3.411E-3	0.7	1.2
45.016	224.3	2178.0	10000	20.0	5.307	75.016	173.3	448.6	0.3864	8447	5129.0698	0.04198	10258	1.0258E6	3.411E-3	0.8	1.3
46.016	228.4	2262.6	10000	20.0	5.287	76.016	180.1	456.8	0.3942	8415	5318.2998	0.04033	10637	1.0637E6	3.411E-3	0.8	1.3
47.020	234.5	2363.9	10000	20.0	5.233	77.020	188.1	469.0	0.4011	8329	5602.4702	0.03786	11205	1.1205E6	3.411E-3	0.8	1.3
48.000	238.5	2433.9	10000	20.0	5.214	78.000	193.7	477.0	0.4060	8298	5800.6001	0.03647	11601	1.1601E6	3.411E-3	0.8	1.3
49.016	242.7	2523.9	10000	20.0	5.172	79.016	200.8	485.3	0.4138	8232	5999.7998	0.03495	12000	1.2000E6	3.411E-3	0.8	1.3
50.000	248.8	2642.3	10000	20.0	5.144	80.000	210.3	497.5	0.4226	8187	6302.5098	0.03308	12605	1.2605E6	3.411E-3	0.8	1.3
51.000	252.8	2723.1	10000	20.0	5.115	81.000	216.7	505.6	0.4286	8141	6510.6401	0.03184	13021	1.3021E6	3.411E-3	0.9	1.4
52.000	259.0	2848.3	10000	20.0	5.054	82.000	226.7	518.1	0.4375	8043	6832.2002	0.02997	13664	1.3664E6	3.411E-3	0.9	1.4
53.000	263.1	2939.1	10000	20.0	5.048	83.000	233.9	526.2	0.4445	8034	7051.2300	0.02902	14102	1.4102E6	3.411E-3	0.9	1.4
54.000	269.1	3083.0	10000	20.0	4.996	84.000	245.3	538.3	0.4558	7951	7374.6499	0.02744	14749	1.4749E6	3.411E-3	0.9	1.4
55.000	273.3	3145.2	10000	20.0	4.967	85.000	250.3	546.5	0.4580	7906	7601.5400	0.02647	15203	1.5203E6	3.411E-3	0.9	1.4
56.000	277.4	3246.3	10000	20.0	4.987	86.000	258.3	554.8	0.4656	7937	7945.3901	0.02579	15891	1.5891E6	3.411E-3	0.9	1.4
57.020	283.4	3394.1	10000	20.0	4.885	87.020	270.1	566.8	0.4766	7775	8169.0698	0.02421	16338	1.6338E6	3.411E-3	1.0	1.5
58.016	287.5	3464.2	10000	20.0	4.845	88.016	275.7	575.0	0.4794	7710	8410.5303	0.02332	16821	1.6821E6	3.411E-3	1.0	1.5
59.000	293.6	3605.7	10000	20.0	4.790	89.000	286.9	587.2	0.4887	7623	8767.6699	0.02211	17535	1.7535E6	3.411E-3	1.0	1.5
60.016	297.6	3711.3	10000	20.0	4.773	90.016	295.3	595.2	0.4962	7596	9007.3496	0.02144	18015	1.8015E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	300.0	3791.0	10000	20.0	4.760	92.004	301.7	600.0	0.5028	7575	295.3340	0.02104	590.67	59067	3.411E-3	0.0	1.5
2.0160	300.0	3780.6	10000	20.0	4.731	93.016	300.8	599.9	0.5015	7530	546.6540	0.02092	1093.3	1.0933E5	3.411E-3	0.0	1.6
3.0280	300.0	3812.7	10000	20.0	4.734	94.028	303.4	600.0	0.5057	7535	925.9770	0.02093	1852.0	1.8520E5	3.411E-3	0.1	1.6
4.0040	300.0	3771.3	10000	20.0	4.756	95.004	300.1	600.0	0.5002	7569	1174.8800	0.02103	2349.8	2.3498E5	3.411E-3	0.1	1.6
5.0280	300.0	3776.8	10000	20.0	4.759	96.028	300.5	600.0	0.5009	7574	1426.4500	0.02104	2852.9	2.8529E5	3.411E-3	0.1	1.6
6.0280	300.0	3759.1	10000	20.0	4.727	97.028	299.1	600.0	0.4985	7523	1803.3300	0.02089	3606.7	3.6067E5	3.411E-3	0.1	1.6
7.0280	300.0	3767.8	10000	20.0	4.736	98.028	299.8	600.0	0.4997	7537	2054.7200	0.02094	4109.4	4.1094E5	3.411E-3	0.1	1.6
8.0280	300.0	3753.9	10000	20.0	4.717	99.028	298.7	600.0	0.4978	7508	2306.1001	0.02085	4612.2	4.6122E5	3.411E-3	0.1	1.7
9.0040	300.0	3787.3	10000	20.0	4.749	100.004	301.4	600.0	0.5023	7559	2683.0400	0.02099	5366.1	5.3661E5	3.411E-3	0.2	1.7
10.000	300.0	3776.4	10000	20.0	4.757	101.000	300.5	600.0	0.5008	7570	2934.3501	0.02103	5868.7	5.8687E5	3.411E-3	0.2	1.7
11.044	300.0	3795.1	10000	20.0	4.738	102.044	302.0	600.0	0.5034	7541	3311.3201	0.02095	6622.6	6.6226E5	3.411E-3	0.2	1.7
12.004	300.0	3792.4	10000	20.0	4.722	103.004	301.8	599.9	0.5030	7516	3562.6699	0.02088	7125.3	7.1253E5	3.411E-3	0.2	1.7
13.028	300.0	3806.8	10000	20.0	4.802	104.028	302.9	600.0	0.5049	7642	3814.0300	0.02123	7628.1	7.6281E5	3.411E-3	0.2	1.7
14.028	300.0	3791.8	10000	20.0	4.732	105.028	301.7	600.0	0.5029	7531	4190.8501	0.02092	8381.7	8.3817E5	3.411E-3	0.2	1.8
15.004	300.0	3768.4	10000	20.0	4.725	106.004	299.9	600.0	0.4998	7520	4442.1499	0.02089	8884.3	8.8843E5	3.411E-3	0.3	1.8
16.036	300.0	3777.4	10000	20.0	4.743	107.036	300.6	600.1	0.5009	7549	4821.3901	0.02097	9642.8	9.6428E5	3.411E-3	0.3	1.8
17.004	300.0	3784.0	10000	20.0	4.731	108.004	301.1	600.0	0.5018	7530	5070.4902	0.02091	10141	1.0141E6	3.411E-3	0.3	1.8
18.028	300.0	3777.2	10000	20.0	4.754	109.028	300.6	600.0	0.5010	7565	5322.0400	0.02102	10644	1.0644E6	3.411E-3	0.3	1.8
19.004	300.0	3735.5	10000	20.0	4.741	110.004	297.3	600.0	0.4954	7546	5699.0000	0.02096	11398	1.1398E6	3.411E-3	0.3	1.8
20.016	300.0	3781.2	10000	20.0	4.735	111.016	300.9	600.0	0.5015	7535	5950.1299	0.02093	11900	1.1900E6	3.411E-3	0.3	1.9
21.028	300.0	3771.2	10000	20.0	4.763	112.028	300.1	600.0	0.5002	7581	6328.6602	0.02106	12657	1.2657E6	3.411E-3	0.4	1.9
22.028	300.0	3778.2	10000	20.0	4.759	113.028	300.7	600.0	0.5011	7575	6579.7402	0.02104	13159	1.3159E6	3.411E-3	0.4	1.9
23.044	300.0	3761.2	10000	20.0	4.708	114.044	299.3	600.0	0.4989	7493	6829.7798	0.02081	13660	1.3660E6	3.411E-3	0.4	1.9
24.008	300.0	3783.6	10000	20.0	4.719	115.008	301.1	600.0	0.5018	7511	7206.9399	0.02086	14414	1.4414E6	3.411E-3	0.4	1.9
25.028	300.0	3772.2	10000	20.0	4.739	116.028	300.2	599.9	0.5004	7543	7458.0801	0.02096	14916	1.4916E6	3.411E-3	0.4	1.9
26.044	300.0	3769.7	10000	20.0	4.717	117.044	300.0	600.0	0.5000	7507	7836.7300	0.02085	15673	1.5673E6	3.411E-3	0.4	2.0
27.004	300.0	3767.9	10000	20.0	4.756	118.004	299.8	600.0	0.4997	7569	8086.4800	0.02102	16173	1.6173E6	3.411E-3	0.5	2.0
28.048	300.0	3806.4	10000	20.0	4.782	119.048	302.9	600.0	0.5048	7611	8338.1201	0.02114	16676	1.6676E6	3.411E-3	0.5	2.0
29.036	300.0	3768.0	10000	20.0	4.738	120.036	299.8	600.0	0.4997	7541	8714.7002	0.02094	17429	1.7429E6	3.411E-3	0.5	2.0
30.004	300.0	3778.2	10000	20.0	4.747	121.004	300.7	600.0	0.5011	7554	8966.1504	0.02098	17932	1.7932E6	3.411E-3	0.5	2.0
31.004	300.0	3783.1	10000	20.0	4.763	122.004	301.1	600.1	0.5017	7581	9220.0400	0.02105	18440	1.8440E6	3.411E-3	0.5	2.0
32.028	300.0	3806.0	10000	20.0	4.752	123.028	302.9	599.9	0.5048	7562	9596.5898	0.02101	19193	1.9193E6	3.411E-3	0.5	2.1
33.028	300.0	3784.6	10000	20.0	4.729	124.028	301.2	600.0	0.5020	7526	9847.0000	0.02091	19694	1.9694E6	3.411E-3	0.6	2.1
34.028	300.0	3814.2	10000	20.0	4.825	125.028	303.5	600.0	0.5059	7679	10224.100	0.02133	20448	2.0448E6	3.411E-3	0.6	2.1
35.032	300.0	3790.7	10000	20.0	4.746	126.032	301.7	600.0	0.5027	7554	10474.200	0.02098	20948	2.0948E6	3.411E-3	0.6	2.1
36.028	300.0	3784.5	10000	20.0	4.732	127.028	301.2	600.0	0.5020	7532	10725.400	0.02092	21451	2.1451E6	3.411E-3	0.6	2.1
37.028	300.0	3782.8	10000	20.0	4.774	128.028	301.0	600.0	0.5017	7598	11106.100	0.02110	22212	2.2212E6	3.411E-3	0.6	2.1
38.028	300.0	3779.6	10000	20.0	4.759	129.028	300.8	600.0	0.5013	7574	11353.900	0.02104	22708	2.2708E6	3.411E-3	0.6	2.2
39.036	300.0	3821.1	10000	20.0	4.741	130.036	304.1	600.0	0.5068	7546	11733.700	0.02096	23467	2.3467E6	3.411E-3	0.7	2.2
40.028	300.0	3791.2	10000	20.0	4.748	131.028	301.7	600.0	0.5028	7557	11982.200	0.02099	23964	2.3964E6	3.411E-3	0.7	2.2
41.028	300.0	3781.6	10000	20.0	4.737	132.028	300.9	599.9	0.5016	7539	12233.400	0.02094	24467	2.4467E6	3.411E-3	0.7	2.2
42.028	300.0	3772.2	10000	20.0	4.725	133.028	300.2	600.0	0.5003	7520	12610.400	0.02089	25221	2.5221E6	3.411E-3	0.7	2.2
43.048	300.0	3785.3	10000	20.0	4.753	134.048	301.2	600.0	0.5021	7564	12861.700	0.02101	25723	2.5723E6	3.411E-3	0.7	2.2
44.004	300.0	3795.8	10000	20.0	4.749	135.004	302.1	600.0	0.5035	7558	13113.000	0.02099	26226	2.6226E6	3.411E-3	0.7	2.3
45.028	300.0	3793.1	10000	20.0	4.694	136.028	301.8	600.0	0.5031	7471	13490.600	0.02075	26981	2.6981E6	3.411E-3	0.8	2.3
46.028	300.0	3778.2	10000	20.0	4.771	137.028	300.7	600.1	0.5010	7594	13741.400	0.02109	27483	2.7483E6	3.411E-3	0.8	2.3
47.036	300.0	3772.2	10000	20.0	4.743	138.036	300.2	600.0	0.5003	7549	14118.800	0.02097	28238	2.8238E6	3.411E-3	0.8	2.3
48.016	300.0	3809.7	10000	20.0	4.763	139.016	303.2	600.0	0.5053	7580	14369.800	0.02106	28740	2.8740E6	3.411E-3	0.8	2.3
49.036	300.0	3776.2	10000	20.0	4.749	140.036	300.5	600.0	0.5008	7559	14621.100	0.02100	29242	2.9242E6	3.411E-3	0.8	2.3
50.028	300.0	3782.1	10000	20.0	4.738	141.028	301.0	600.0	0.5016	7540	14997.900	0.02094	29996	2.9996E6	3.411E-3	0.8	2.4
51.028	300.0	3780.7	10000	20.0	4.725	142.028	300.9	600.0	0.5014	7520	15249.200	0.02089	30498	3.0498E6	3.411E-3	0.9	2.4
52.028	300.0	3793.7	10000	20.0	4.769	143.028	301.9	600.0	0.5031	7590	15629.600	0.02108	31259	3.1259E6	3.411E-3	0.9	2.4
53.004	300.0	3799.1	10000	20.0	4.751	144.004	302.3	600.0	0.5039	7562	15877.600	0.02101	31755	3.1755E6	3.411E-3	0.9	2.4
54.004	300.0	3808.2	10000	20.0	4.751	145.004	303.0	600.1	0.5050	7562	16129.000	0.02100	32258	3.2258E6	3.411E-3	0.9	2.4
55.028	300.0	3773.3	10000	20.0	4.726	146.028	300.3	599.9	0.5005	7521	16505.900	0.02090	33012	3.3012E6	3.411E-3	0.9	2.4
56.028	300.0	3765.7	10000	20.0	4.711	147.028	299.7	600.0	0.4994	7498	16763.699	0.02083	33527	3.3527E6	3.411E-3	0.9	2.5
57.024	300.0	3768.0	10000	20.0	4.734	148.024	299.8	600.0	0.4998	7534	17009.100	0.02093	34018	3.4018E6	3.411E-3	1.0	2.5
58.028	300.0	3802.8	10000	20.0	4.740	149.028	302.6	600.0	0.5044	7544	17385.699	0.02096	34771	3.4771E6	3.411E-3	1.0	2.5
59.028	300.0	3775.9	10000	20.0	4.730	150.028	300.5	600.0	0.5008	7529	17636.900	0.02092	35274	3.5274E6	3.411E-3	1.0	2.5
60.028	300.0	3795.1	10000	20.0	4.780	151.028	302.0	600.0	0.5034	7607	18013.900	0.02113	36028	3.6028E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99200	297.3	3707.9	10000	20.0	4.749	151.992	295.1	594.7	0.4962	7559	250.0520	0.02137	500.10	50010	3.411E-3	0.0	2.5
2.0120	291.3	3588.6	10000	20.0	4.827	153.012	285.6	582.7	0.4901	7682	607.1220	0.02263	1214.2	1.2142E5	3.411E-3	0.0	2.6
3.0120	287.3	3485.6	10000	20.0	4.819	154.012	277.4	574.5	0.4828	7670	845.0630	0.02324	1690.1	1.6901E5	3.411E-3	0.1	2.6
3.9960	283.1	3380.0	10000	20.0	4.917	154.996	269.0	566.3	0.4750	7825	1082.9301	0.02440	2165.9	2.1659E5	3.411E-3	0.1	2.6
4.9960	277.1	3261.1	10000	20.0	4.913	155.996	259.5	554.2	0.4683	7819	1421.1400	0.02546	2842.3	2.8423E5	3.411E-3	0.1	2.6
5.9960	273.1	3159.5	10000	20.0	4.958	156.996	251.4	546.1	0.4604	7891	1646.5200	0.02646	3293.0	3.2930E5	3.411E-3	0.1	2.6
7.0120	266.8	3006.9	10000	20.0	5.003	158.012	239.3	533.7	0.4484	7963	1984.6500	0.02796	3969.3	3.9693E5	3.411E-3	0.1	2.6
7.9960	262.8	2941.8	10000	20.0	5.035	158.996	234.1	525.6	0.4454	8013	2197.6101	0.02900	4395.2	4.3952E5	3.411E-3	0.1	2.6
8.9960	256.7	2812.5	10000	20.0	5.085	159.996	223.8	513.4	0.4359	8093	2519.0000	0.03070	5038.0	5.0380E5	3.411E-3	0.1	2.7
9.9960	252.6	2711.6	10000	20.0	5.112	160.996	215.8	505.2	0.4271	8136	2731.0801	0.03188	5462.2	5.4622E5	3.411E-3	0.2	2.7
10.992	248.4	2637.1	10000	20.0	5.116	161.992	209.9	496.9	0.4223	8143	2937.6201	0.03298	5875.2	5.8752E5	3.411E-3	0.2	2.7
12.000	242.4	2522.7	10000	20.0	5.177	163.000	200.7	484.8	0.4141	8240	3236.6799	0.03507	6473.4	6.4734E5	3.411E-3	0.2	2.7
12.996	238.2	2449.4	10000	20.0	5.204	163.996	194.9	476.5	0.4091	8283	3442.7400	0.03648	6885.5	6.8855E5	3.411E-3	0.2	2.7
14.008	232.1	2335.4	10000	20.0	5.243	165.008	185.8	464.3	0.4003	8345	3725.2100	0.03871	7450.4	7.4504E5	3.411E-3	0.2	2.8
14.996	228.1	2260.6	10000	20.0	5.273	165.996	179.9	456.2	0.3943	8392	3913.0901	0.04033	7826.2	7.8262E5	3.411E-3	0.2	2.8
15.996	221.9	2137.3	10000	20.0	5.300	166.996	170.1	443.8	0.3833	8436	4196.2402	0.04284	8392.5	8.3925E5	3.411E-3	0.3	2.8
17.012	217.7	2062.6	10000	20.0	5.322	168.012	164.1	435.5	0.3769	8471	4375.6401	0.04467	8751.3	8.7513E5	3.411E-3	0.3	2.8
18.012	213.7	1989.4	10000	20.0	5.356	169.012	158.3	427.4	0.3704	8525	4550.8101	0.04666	9101.6	9.1016E5	3.411E-3	0.3	2.8
18.996	207.5	1864.4	10000	20.0	5.381	169.996	148.4	415.1	0.3574	8565	4813.3101	0.04972	9626.6	9.6266E5	3.411E-3	0.3	2.8
19.996	203.3	1825.9	10000	20.0	5.417	170.996	145.3	406.7	0.3573	8622	4988.6201	0.05213	9977.3	9.9773E5	3.411E-3	0.3	2.8
20.996	197.2	1693.4	10000	20.0	5.445	171.996	134.8	394.5	0.3416	8666	5233.6699	0.05570	10467	1.0467E6	3.411E-3	0.3	2.9
22.000	193.1	1625.0	10000	20.0	5.460	173.000	129.3	386.2	0.3349	8689	5395.0698	0.05826	10790	1.0790E6	3.411E-3	0.4	2.9
22.996	188.9	1556.9	10000	20.0	5.479	173.996	123.9	377.7	0.3280	8720	5558.6899	0.06111	11117	1.1117E6	3.411E-3	0.4	2.9
23.996	182.8	1459.9	10000	20.0	5.509	174.996	116.2	365.6	0.3178	8768	5782.4800	0.06560	11565	1.1565E6	3.411E-3	0.4	2.9
25.000	178.7	1390.3	10000	20.0	5.529	176.000	110.6	357.4	0.3096	8799	5932.5601	0.06890	11865	1.1865E6	3.411E-3	0.4	2.9
25.996	174.5	1324.9	10000	20.0	5.557	176.996	105.4	348.9	0.3021	8845	6159.3599	0.07264	12319	1.2319E6	3.411E-3	0.4	2.9
27.000	168.3	1246.5	10000	20.0	5.589	178.000	99.19	336.5	0.2948	8895	6295.5898	0.07855	12591	1.2591E6	3.411E-3	0.5	3.0
27.996	164.2	1176.1	10000	20.0	5.602	178.996	93.59	328.3	0.2851	8917	6432.2998	0.08272	12865	1.2865E6	3.411E-3	0.5	3.0
29.012	157.8	1078.5	10000	20.0	5.627	180.012	85.83	315.7	0.2719	8955	6638.5000	0.08988	13277	1.3277E6	3.411E-3	0.5	3.0
29.996	153.7	1019.5	10000	20.0	5.640	180.996	81.13	307.5	0.2638	8976	6763.3501	0.09492	13527	1.3527E6	3.411E-3	0.5	3.0
30.996	147.6	982.76	10000	20.0	5.663	181.996	78.21	295.2	0.2649	9012	6951.2598	0.1034	13903	1.3903E6	3.411E-3	0.5	3.0
32.012	143.4	886.43	10000	20.0	5.674	183.012	70.54	286.7	0.2460	9031	7075.4902	0.1099	14151	1.4151E6	3.411E-3	0.5	3.1
32.996	139.1	847.38	10000	20.0	5.698	183.996	67.43	278.2	0.2424	9069	7193.9702	0.1172	14388	1.4388E6	3.411E-3	0.5	3.1
33.996	132.9	773.98	10000	20.0	5.715	184.996	61.59	265.9	0.2316	9096	7363.4199	0.1287	14727	1.4727E6	3.411E-3	0.6	3.1
35.012	128.7	725.45	10000	20.0	5.732	186.012	57.73	257.4	0.2243	9123	7474.7598	0.1377	14950	1.4950E6	3.411E-3	0.6	3.1
35.996	124.4	684.99	10000	20.0	5.739	186.996	54.51	248.9	0.2190	9134	7580.7402	0.1475	15161	1.5161E6	3.411E-3	0.6	3.1
36.996	118.3	622.82	10000	20.0	5.750	187.996	49.56	236.7	0.2094	9151	7730.2900	0.1634	15461	1.5461E6	3.411E-3	0.6	3.1
37.996	114.1	579.24	10000	20.0	5.763	188.996	46.09	228.2	0.2020	9172	7829.9800	0.1762	15660	1.5660E6	3.412E-3	0.6	3.1
39.004	109.7	542.81	10000	20.0	5.777	190.004	43.20	219.4	0.1969	9195	7929.5400	0.1911	15859	1.5859E6	3.412E-3	0.7	3.2
40.000	103.5	491.93	10000	20.0	5.780	191.000	39.15	206.9	0.1892	9199	8060.3999	0.2149	16121	1.6121E6	3.411E-3	0.7	3.2
41.000	99.19	456.06	10000	20.0	5.790	192.000	36.29	198.4	0.1829	9215	8147.4199	0.2342	16295	1.6295E6	3.411E-3	0.7	3.2
42.000	94.75	418.28	10000	20.0	5.795	193.000	33.29	189.5	0.1757	9223	8234.4404	0.2569	16469	1.6469E6	3.411E-3	0.7	3.2
42.996	88.54	374.93	10000	20.0	5.810	193.996	29.84	177.1	0.1685	9248	8346.3604	0.2949	16693	1.6693E6	3.411E-3	0.7	3.2
43.996	84.27	345.23	10000	20.0	5.812	194.996	27.47	168.5	0.1630	9251	8420.7998	0.3257	16842	1.6842E6	3.411E-3	0.7	3.2
45.008	79.77	316.53	10000	20.0	5.818	196.008	25.19	159.5	0.1579	9260	8495.2100	0.3638	16990	1.6990E6	3.411E-3	0.8	3.3
45.996	75.22	282.66	10000	20.0	5.824	196.996	22.49	150.4	0.1495	9269	8563.4502	0.4096	17127	1.7127E6	3.411E-3	0.8	3.3
47.008	68.82	242.88	10000	20.0	5.830	198.008	19.33	137.6	0.1404	9279	8656.5898	0.4897	17313	1.7313E6	3.411E-3	0.8	3.3
48.008	64.22	216.39	10000	20.0	5.835	199.008	17.22	128.4	0.1341	9286	8718.1201	0.5629	17436	1.7436E6	3.411E-3	0.8	3.3
48.992	59.53	191.06	10000	20.0	5.845	199.992	15.20	119.1	0.1277	9302	8773.6396	0.6562	17547	1.7547E6	3.411E-3	0.8	3.3
49.996	55.27	170.56	10000	20.0	5.847	200.996	13.57	110.5	0.1228	9305	8822.9902	0.7615	17646	1.7646E6	3.411E-3	0.8	3.3
50.996	50.66	143.97	10000	20.0	5.853	201.996	11.46	101.3	0.1131	9315	8872.1904	0.9072	17744	1.7744E6	3.411E-3	0.8	3.4
52.012	43.92	114.90	10000	20.0	5.859	203.012	9.144	87.83	0.1041	9326	8933.5996	1.209	17867	1.7867E6	3.411E-3	0.9	3.4
52.996	39.55	96.056	10000	20.0	5.863	203.996	7.644	79.09	0.09664	9331	8970.3203	1.492	17941	1.7941E6	3.411E-3	0.9	3.4
54.012	34.66	76.852	10000	20.0	5.869	205.012	6.116	69.32	0.08822	9341	9006.8398	1.944	18014	1.8014E6	3.411E-3	0.9	3.4
55.016	29.53	58.137	10000	20.0	5.871	206.016	4.626	59.06	0.07834	9345	9037.0801	2.679	18074	1.8074E6	3.411E-3	0.9	3.4
55.992	25.13	44.952	10000	20.0	5.871	206.992	3.577	50.27	0.07116	9345	9061.1904	3.698	18122	1.8122E6	3.411E-3	0.9	3.4
57.012	19.88	30.308	10000	20.0	5.873	208.012	2.412	39.76	0.06066	9348	9085.0303	5.912	18170	1.8170E6	3.411E-3	1.0	3.5
57.996	13.97	17.244	10000	20.0	5.877	208.996	1.372	27.94	0.04912	9354	9102.2402	11.98	18204	1.8204E6	3.411E-3	1.0	3.5
58.996	11.71	12.990	10000	20.0	5.874	209.996	1.034	23.42	0.04415	9349	9107.9004	17.05	18216	1.8216E6	3.411E-3	1.0	3.5
60.012	6.466	4.1664	10000	20.0	5.878	211.012	0.3315	12.93	0.02564	9355	9116.0195	55.94	18232	1.8232E6	3.411E-3	1.0	3.5

